Preparation of copper and nickel based nanoparticles by magnetron sputtering and their use in sulfur–sulfur bond activation reaction

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The present work is devoted to a systematic study of the advantages and limitations of the magnetron sputtering method, which is a convenient and promising way to obtain nanosized particles directly from the bulk metal, when it is used to prepare nanoparticles of the first-row transition metals. In the course of the study, variation of sputtering media based on ionic liquids, eutectic solvents, low and high molecular weight organic compounds was carried out. Particles of copper, nickel, a copper-nickel alloy and a copper-zinc alloy were obtained. Using the example of the activation reaction of the sulfur–sulfur bond in diphenyl disulfide, it has been shown that up to 96% of the sputtered copper can be effectively used in catalysis, whereas in the case of nickel and zinc about three quarters of the metal can be converted to an inactive form, at the same time readily oxidizable components can act as sacrificial stabilizers for moderately active metal particles in sputtering two-component alloys.

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作者简介

А. Kashin

N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences

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Email: a.kashin@ioc.ac.ru
俄罗斯联邦, 119991, Moscow

参考

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2. Table 1

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3. Fig. 1. (a) Schematic diagram of the magnetron sputtering device. M(0) is a metal in the zero oxidation state. (b) Liquids used as a medium. Liquids that are compatible with the vacuum of the sputtering chamber but interact with the sputtered particles are marked in red; inert stable media suitable for use in the synthesis of nanoparticles are marked in green.

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4. Fig. 2. Energy-dispersive X-ray spectra in the 2–3 keV and 7–10 keV ranges for samples of the metal-containing phase isolated after the reaction between diphenyl disulfide and particles of copper (black curve), nickel (red curve), copper-nickel alloy (blue curve) or copper-zinc alloy (green curve) in a pyridinium ionic liquid medium.

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5. Fig. 3. STEM images of copper and copper-zinc alloy particles in a pyridinium ionic liquid medium (a) and (d) and the corresponding histograms of particle size distribution (b) and (d); STEM images of reaction mixtures obtained after treating copper and copper-zinc alloy particles with diphenyl disulfide in an ionic liquid medium (c) and (e).

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Represented by Academician of the RAS V.P. Ananikov


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